Crystal structure of 1 -adamantylammonium 4-nitrophenolate hydrate, (C10H15NH3)(OC6H4NO2) · H2O
Year: 2004
Type: article
Abstract: C16H24N2O4, monoclinic, P\2\ln\ (no.14), a = 6.433(4)A, b = 11.366(2)A, e = 22.406(3) A, P = 94.77(4)°,V = 1632.6A 3 , Z = 4, RgtF) = 0.057, wR^F 1 ) = 0.144, T= 293 K.Source of material 13.9 g (0.1 mol) 4-nitrophenol and 1.51 g (0.1 mol) 1 -adamantanamine were weighted, respectively, and mixed with 20 mL ethanol and 10 mL water together, and then heated until the solid had dissolved completely.After cooling gradually and standing still at room temperature for a few days, the white crystalline solid suitable for X-ray diffraction were obtained.
Authors: W.-S. Guo, F. Guo
Institution: Liaoning University
Language: German
Subfield: Inorganic Chemistry
Field: Chemistry
Domain: Physical Sciences
Open Access status: gold
Estimated APC paid: $848
OpenAlex ID: W2044757323