Work

Crystal structure of (2R,4S,5R)-2-(4-benzyloxy-5-benzyloxymethyltetrahydrofuranyl) triphenylphosphonium tetrafluoroborate tetrachloromethane solvate, C37H36PBF4O3 CCI4

Year: 1998

Type: article

Abstract: Source of material: The title compound was prepared by reaction of methyl 3,5-di-0-benzyl-2,3-dideoxy-D-ribofuranoside with hydrogentriphenylphosphonium tetrafluoroborate in acetonitrile. The precipitated phosphonium salt was recrystallized from tetrachloromethane/dichloromethane. \nOne tetrachloromethane solvent molecule per asymmetric unit was found. This solvent molecule was strongly disordered.

Source: Zeitschrift für Kristallographie - New Crystal Structures

DOI: 10.1524/ncrs.1998.213.14.379

Authors: W. Frey, A. Lieberknecht, H. Griesser, R. D. Bravo, P. A. Colinas, R. J. Grigera

Institutions: University of Stuttgart, Instituto de Fisica de Liquidos y Sistemas Biologicos, Universidad Nacional de La Plata

Language: German

Topic: Crystal structures of chemical compounds

Subfield: Inorganic Chemistry

Field: Chemistry

Domain: Physical Sciences

Open Access status: gold

Estimated APC paid: $848

Funders: Deutscher Akademischer Austauschdienst, Consejo Nacional de Investigaciones Científicas y Técnicas