Work

Estimation of directional single crystal elastic properties from nano-indentation by correlation with EBSD and first-principle calculations

Year: 2023

Type: article

Abstract: In this study, a two-step optimisation process for the estimation of the single crystal stiffness tensor from the indentation modulus is presented. This was accomplished by using a 2-dimensional data correlation method for nano-indentation, EBSD and ab initio data, as well as EDS for phase separation in a multi-phase material. Here, a single-phase Fe-24Ni-0.4C austenitic steel and a two-phase Fe-9Ni-0.5Co Seymchan meteorite were used as example materials. In a first step, the combination of high-speed nano-indentation mapping data with elemental and orientation distribution maps allowed the prediction of indentation moduli along specific crystal surface planes normal directions, (0 0 1), (0 1 1) and (1 1 1) using a least squares optimisation based on starting values from DFT or experimentally determined stiffness tensors. A second global optimisation step to estimate the single crystal stiffness tensor using pre-solved solution parameters of the Vlassak-Nix equations yielded reasonable correspondence between the experimentally determined stiffness tensors from correlative nano-indentation data and other methods. The presented method demonstrates generally the possibility to derive directionally sensitive elastic properties from high-speed nano-indentation for cubic materials statistically.

Source: Materials & Design

DOI: 10.1016/j.matdes.2023.112296

Authors: Mattis Seehaus, Sang-Hyeok Lee, Tobias Stollenwerk, Jeffrey M. Wheeler, Sandra Korte-Kerzel

Institutions: RWTH Aachen University, ETH Zurich

Language: English

Topic: Metal and Thin Film Mechanics

Subfield: Mechanics of Materials

Field: Engineering

Domain: Physical Sciences

Open Access status: gold

Estimated APC paid: $2,800