In situ decorated pd NPs on Triazin-encapsulated Fe3O4/SiO2-NH2 as magnetic catalyst for the synthesis of diaryl ethers and oxidation of sulfides
Year: 2024
Type: article
Abstract: This article is devoted to the synthesis of a new magnetic palladium catalyst that has been immobilized on A-TT-Pd coated-magnetic Fe3O4 nanoparticles. Such surface functionalization of magnetic particles is a promising method to bridge the gap between heterogeneous and homogeneous catalysis approaches. The structure, morphology, and physicochemical properties of the particles were characterized through different analytical techniques, including TEM, FT-IR, XRD, SEM, EDS, TGA-DTG, ICP, and VSM techniques. The obtained Fe3O4@SiO2@A-TT-Pd performance can show excellent catalytic activity for the synthesis of diaryl ethers and oxidation of sulfides, and the corresponding products were obtained with high yields. The advantages of this catalyst include a simple test method, green reaction conditions, no use of dangerous solvents, short reaction time, low catalyst loading, and reusability. Also, the nanocatalyst was easily separated from the reaction mixture with the help of a bar magnet and recovered and reused several times without loss of stability and activity.
Source: Scientific Reports
Authors: Durgesh Singh, Kamini Singh, Pawan Sharma, Yashwantsinh Jadeja, Johar MGM, Priyanka Singh, Kiranjeet Kaur, M. Atif, Mohammed A. El-Meligy, Beneen Husseen
Institutions: Dr. Hari Singh Gour University, Deen Dayal Upadhyaya Gorakhpur University, Jain University, Vivekananda Global University, Marwadi University, Management and Science University, NIMS University, Chandigarh University, King Saud University, Applied Science Private University, Jadara University, Islamic University of Najaf
Language: English
Subfield: Organic Chemistry
Field: Chemistry
Domain: Physical Sciences
Open Access status: gold
Estimated APC paid: $2,590
Funder: King Saud University
Award: G2872084949
OpenAlex ID: W4403714414