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Bis(N-Alkyl-N-diphenylphosphinylmethyl)diglycolamides: Synthesis and NMR Spectroscopy Study

Year: 2024

Type: article

Abstract: Bis(N-Alkyl-N-diphenylphosphinylmethyl)diglycolamides [Ph2P(O)CH2N(R)C(O)CH2]2O, where R = Et, i-Pr, n-Bu, i-Bu, n-Oct, were synthesized by reaction of diglycolyl chloride with N-alkyl-N-(diphenylphosphinylmethyl)amines Ph2P(O)CH2NHR obtained by the Kabachnik–Fields reaction of aminomethylation of diphenylphosphinous acid, and their hydrochlorides. The structure of the obtained compounds was studied by 1H, 13C and 31P NMR spectroscopy.

Source: Журнал Общей Химии

DOI: 10.31857/s0044460x24070046

Authors: O. I. Artyushin, E. V. Sharova, K. V. Tcarkova, A. S. Peregudov, N. A. Bondarenko

Institutions: A. N. Nesmeyanov Institute of Organoelement Compounds, Kurchatov Institute

Language: English

Topic: Organophosphorus compounds synthesis

Subfield: Organic Chemistry

Field: Chemistry

Domain: Physical Sciences

Open Access status: bronze

OpenAlex ID: W4405622168

FWCI:

Cites: 24

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Related to: 10