synthesis and characterization of 1,2,4-traiazole derivative from methyl benzaoate with sulfur bridge links
Year: 2024
Type: article
Abstract: The basic nucleus S-(4-(((E)-benzylidene)amino)-5-phenyl-4H-1,2,4-triazol-3-yl) 2-((4-(((E)-benzylidene)amino)-5-phenyl-4H-1,2,4-triazol-3-yl)thio) ethanethioate T.4 produced with many steps, from the cyclization of T.2 with carbon disulfide/ potassium hydroxide using ethanol as a solvent followed by the addition of hydrazine hydrate for 12 hours while experiencing reflux. To create the Schiff base T.3, the successfully synthesized by reflux of T.2 with 1,4-dicarbaldehyde then react T.3 with chemical was exposed to condensation with chloroacetyl chloride. Physical characteristics, such as the melting point, and spectroscopic analysis were used to confirm the compounds (FT-IR) and (1H- NMR).The basic nucleus S-(4-(((E)-benzylidene)amino)-5-phenyl-4H-1,2,4-triazol-3-yl) 2-((4-(((E)-benzylidene)amino)-5-phenyl-4H-1,2,4-triazol-3-yl)thio) ethanethioate T.4 produced with many steps, from the cyclization of T.2 with carbon disulfide/ potassium hydroxide using ethanol as a solvent followed by the addition of hydrazine hydrate for 12 hours while experiencing reflux. To create the Schiff base T.3, the successfully synthesized by reflux of T.2 with 1,4-dicarbaldehyde then react T.3 with chemical was exposed to condensation with chloroacetyl chloride. Physical characteristics, such as the melting point, and spectroscopic analysis were used to confirm the compounds (FT-IR) and (1H- NMR).
Authors: Ahmed Ahmed, Noor Tariq, Waled Abdo Ahmed, Amamer Redwan
Institutions: Nahrain University, Bani-Waleed University
Language: English
Subfield: Organic Chemistry
Field: Chemistry
Domain: Physical Sciences
Open Access status: diamond
Funder: Al-Nahrain University
OpenAlex ID: W4406434097