Work

Synthesis and crystal structure analysis of substituted bicyclo[3.3.1]nonanones

Year: 2025

Type: article

Abstract: A set of novel bicyclo[3.3.1]nonanones, namely, 4-methoxybicyclo[3.3.1]non-3-ene-2,9-dione, C10H12O3 (1), 4,9,9-trimethoxybicyclo[3.3.1]non-3-en-2-ol, C12H20O4 (2), 4-methoxy-6-methyl-1-(3-methylbut-2-en-1-yl)-6-(4-methylpent-3-en-1-yl)bicyclo[3.3.1]non-3-ene-2,9-dione, C22H32O3 (3) and 4-(tert-butyl)-4-hydroxy-2-methoxy-8-methyl-7-(3-methylbut-2-en-1-yl)-8-(4-methylpent-3-en-1-yl)bicyclo[3.3.1]non-2-en-9-one, C26H42O3 (4), were synthesized and structurally elucidated by NMR, HRMS and X-ray crystallography.

Source: Acta Crystallographica Section E Crystallographic Communications

DOI: 10.1107/s2056989025003299

Authors: Julien A. König, Bernd Morgenstern, Johann Jauch

Institution: Saarland University

Language: English

Topic: Crystal structures of chemical compounds

Subfield: Inorganic Chemistry

Field: Chemistry

Domain: Physical Sciences

Open Access status: gold

Estimated APC paid: $500

Funders: Deutsche Forschungsgemeinschaft, Universität des Saarlandes