Investigation of the interaction conditions of As2S5 and CuCl2 compounds in water and ethylene glycol medium
Year: 2025
Type: article
Abstract: The article presents the results of interaction conditions of CuCl2 and As2S5 in ethylene glycol and aquatic medium. Besides, results of the obtained samples' physicochemical properties are given by X-ray diffraction (XRD), differential thermogravimetric (DTG), thermogravimetric (TG), elemental and scanning electron microscope (SEM) methods. It was found that when ethylene glycol and water are used as a solvent and CuCl2 and As2S5 as the initial components, Cu3AsS4 is obtained at a temperature of 323-353 K. According to the results of DTA analysis, it was found that the melting point of obtained samples was 964.4 K contrary to the reactions carried out to obtain Cu3(AsS4)2 compounds both in ethylene glycol and water medium. Elemental analysis of the compounds was carried out, energy-dispersion spectrum, mass, and atomic ratios of copper, arsenic, and sulfur were determined, and the stoichiometric composition of Cu3AsS4 was determined. Furthermore, X-ray analysis of the obtained samples confirmed that peaks on the graphs correspond to the standard intensity maxima of the Cu3AsS4 compound.
Source: TURKISH JOURNAL OF CHEMISTRY
Authors: HUSEYN IMANOV, MAHNUR JAFARLI
Institutions: Nakhchivan University, Nakhchivan State University
Language: English
Field: Materials Science
Domain: Physical Sciences
Open Access status: diamond
OpenAlex ID: W4409740844