Work

Phase Transformation Kinetics During Post-Weld Heat Treatment in Weldments of C-250 Maraging Steel

Year: 2025

Type: article

Abstract: Welding of maraging steels leads to a microstructural gradient from base material (BM) to weld metal (WM). During post-weld heat treatment (PWHT) the precipitation and reverted austenite (γr) reactions will occur defining the mechanical properties. These reactions are affected by the microstructure and local chemical composition of each zone in the “as welded” (AW) condition. This effect has not been clearly described yet nor the evolution of the microstructure. The objective of this work was to analyse the phase transformations at the different zones of the welded joint during the PWHT to explain the microstructure obtained at each zone. Samples of C250 maraging steel were butt-welded by GTAW-P (Gas Tungsten Arc Welding—Pulsed) process without filler material. The AW condition showed an inhomogeneous microhardness profile, associated with a partial precipitation hardening in the subcritical heat affected zone (SC-HAZ) followed by a softening in the intercritical (IC-HAZ) and recrystallized heat affected zone (R-HAZ). A loop-shaped phase was observed between low temperature IC-HAZ and SC-HAZ, associated with γr, as well as microsegregation at the weld metal (WM). The microstructural evolution during PWHT (480 °C) was evaluated on samples treated to different times (1–360 min). Microhardness profile along the welded joint was mostly homogeneous after 5 min of PWHT due to precipitation reaction. The microhardness in the WM was lower than in the rest of the joint due to the depletion of Ni, Ti and Mo in the martensite matrix related with the γr formation. The isothermal kinetics of precipitation reaction at 480 °C was studied using Differential Scanning Calorimetry (DSC), obtaining a JMAK expression. The average microhardness for each weld zone was proposed for monitoring the precipitation during PWHT, showing a different behaviour for the WM. γr in the WM was also quantified and modelled, while in the IC-HAZ tends to increase with PWHT time, affecting the microhardness.

Source: Materials

DOI: 10.3390/ma18122820

Authors: Mercedes Andrea Duran, Pablo Peitsch, Hernán Gabriel Svoboda

Institutions: Universidad de Buenos Aires, Universidad Nacional de Hurlingham, Comisión Nacional de Energía Atómica, Consejo Nacional de Investigaciones Científicas y Técnicas

Language: English

Topic: Microstructure and Mechanical Properties of Steels

Subfield: Mechanical Engineering

Field: Engineering

Domain: Physical Sciences

Open Access status: gold

Estimated APC paid: $3,137

Funders: Comisión Nacional de Energía Atómica, Gobierno de Argentina, Consejo Nacional de Investigaciones Científicas y Técnicas