Work

Hydrogen bonding in the crystal structure of the organic salt ( R )-1-phenylethan-1-aminium ( R )-5-(1,2-dithiolan-3-yl)pentanoate – a salt of the lipoic acid

Year: 2025

Type: article

Abstract: C 16 H 25 NO 2 S 2 , monoclinic, P 2 1 (no. 4), a = 10.8352(3) Å, b = 6.3694(2) Å, c = 13.3196(4) Å, β = 107.681(4)°, Z = 2, V = 875.81(5) Å 3 , R gt ( F ) = 0.0233, w R ref = 0.0525, Flack–Parsons-parameter: −0.002(6) using 1518 quotients [(I+)−(I−)]/[(I+)+(I−)] (Parsons, S.; Flack, H. D.; Wagner, T. Use of Intensity Quotients and Differences in Absolute Structure Refinement. Acta Crystallogr. 2013 , B69, 249–259), T = 150(2) K.

Source: Zeitschrift für Kristallographie - New Crystal Structures

DOI: 10.1515/ncrs-2025-0358

Author: Guido J. Reiss

Institution: Heinrich Heine University Düsseldorf

Language: English

Topic: Crystal structures of chemical compounds

Subfield: Inorganic Chemistry

Field: Chemistry

Domain: Physical Sciences

Open Access status: gold

Estimated APC paid: $848

Funder: Deutsche Forschungsgemeinschaft