Automated columnar microstructure analysis using CoCo (Column Counter): Insights from EB-PVD TBCs
Year: 2025
Type: article
Abstract: Thermal barrier coatings (TBCs) are essential for protecting gas turbine components from extreme heat. The columnar microstructures produced by conventional electron beam physical vapour deposition (EB-PVD) provide pathways for the transport of heat and molten calcium–magnesium–alumino–silicates (CMAS), compromising their insulation capability and durability. Modifications to the columnar grain morphology have been shown to improve the performance and durability of EB-PVD TBCs, but replicable quantification of these key morphologic parameters remains elusive. In the present work, we present an automated method for the measurement of column width, Column Counter (CoCo). This method is applied to characterize a wide array of microstructures produced by systematically varying substrate temperature (430–1030 °C) and rotation speed (1–8 rpm). The wide spectrum of novel microstructures produced, ranging from columns with periodic porosity bands to layered architectures, markedly diverge from standard columnar TBCs. The morphological analysis is complemented by advanced characterization via X-ray diffraction (XRD) and electron backscattered diffraction (EBSD), revealing how the deposition parameters control column width, crystallographic texture strength and grain multiplicity within columns. Lower temperatures and slower rotations promote finer, less strongly textured coatings with reduced intercolumnar pathways. The results obtained through CoCo showcase the potential of automated morphological analysis in the tailored design of TBCs for improved performance and durability. • Column Counter (CoCo) precisely quantifies column width using BSE and EBSD images. • EB-PVD produces varied TBC microstructures through temperature and rotation control. • Lower temperatures and slower rotation yield finer intercolumnar pores. • EBSD analysis shows TBC columns consist of multiple crystallographic grains. • Quantifying microstructures accelerates the design of highly durable coatings.
Source: Surface and Coatings Technology
Authors: Koldo Almandoz Forcén, Luis Isern, Alan Johnstone, Gyaneshwara Brewster, John Rayment Nicholls, Christine Chalk
Institutions: Cranfield University, Rolls-Royce (United Kingdom)
Language: English
Subfield: Aerospace Engineering
Field: Engineering
Domain: Physical Sciences
Open Access status: hybrid
Estimated APC paid: $3,880
OpenAlex ID: W4416716158