Work

Crystal structure of racemic [(1 R ,2 S ,3 R ,4 S ,6 S )-2,6-bis(furan-2-yl)-4-hydroxy-4-(thiophen-2-yl)cyclohexane-1,3-diyl]bis(thiophen-2-ylmethanone)

Year: 2016

Type: article

Abstract: In the title compound, C28H22O5S3, the central cyclo-hexane ring adopts a chair conformation. The atoms of the furan ring attached to the 6-position of the central cyclo-hexane ring are disordered over two sets of sites with occupancies of 0.832 (5) and 0.168 (5). The hy-droxy group is disordered over two positions (at the 4- and 6-positions of the cyclo-hexane ring) in the ratio 0.832 (5):0.168 (5). In the crystal, mol-ecules are linked by C-H⋯O hydrogen bonds and C-H⋯π inter-actions, forming layers parallel to (100).

Source: Acta Crystallographica Section E Crystallographic Communications

DOI: 10.1107/s2056989016009452

Authors: Ísmail Çelik, Cem Cüneyt Ersanlı, Mehmet Akkurt, Hayrettin Gezegen, Rahmi Köseoğlu

Institutions: Sivas Cumhuriyet Üniversitesi, Sinop University, Erciyes University

Language: English

Topic: Crystal structures of chemical compounds

Subfield: Inorganic Chemistry

Field: Chemistry

Domain: Physical Sciences

Open Access status: gold

Estimated APC paid: $500

Funder: Sinop Üniversitesi