Application of the QuEChERS Method for the Analysis of Contamination by Pesticide Residues in the Sediments of Three Moroccan lagoons
Year: 2023
Type: article
Abstract: Agricultural, industrial, and domestic activities are major contributors to the contamination of natural environments.The aim of this study is to assess the level of sediment contamination by organic pollutants in three Moroccan lagoons: Moulay Bousselham, Oualidia, and Khnifiss.samples were analyzed using liquid chromatography (LC) coupled with mass spectrometry (MS) in Multiple Reaction Monitoring (MRM) mode to detect organophosphorus, carbamate, urea and its derivatives, and other chemical groups.Gas chromatography (GC) coupled with mass spectrometry (MS) was also used to analyze organochlorines.The samples were subjected to dispersive solid-phase extraction (dSPE) using QuEChERS before analysis.Fifteen active substances were detected, including organochlorines, organophosphates, carbamates, ureas, pyrethroids, and others.Three active substances, known for their high toxicity in aquatic environments (carbendazim, malathion, and chlorpyrifos), were identified.The heptachlor molecule (organochlorine family), although banned in Morocco, was still detected in the sediments of the lagoons of Oualidia and Khenifiss.Given the potential harm that these pesticides can cause to living organisms, it is crucial to introduce new crop protection techniques to address this issue.
Authors: Rachida Fegrouche, Hicham Dahak, Taha El Kamli, Mohammed Oussekour, Saida Zaza, Abdelkrim Ben Salem, Badreddine Benyacoub
Language: English
Subfield: Food Science
Domain: Life Sciences
Open Access status: gold
Estimated APC paid: $330
OpenAlex ID: W4388320373